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SIGRAY QuantumLeap-V210 X-ray Absorption Spectroscopy (XAS) system
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SIGRAY TriLambaXRM-30 3D nano x-ray microscope with 35nm resolution
SIGRAY TriLambaXRM-30

SIGRAY QuantumLeap-V210

The QuantumLeap is the first laboratory X-ray absorption spectroscopy (XAS) with synchrotron-like performance to provide critical information on oxidation states, bond lengths and interatomic distances, electron symmetry, and more.

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  • Description
Description

The SIGRAY QuantumLeap-V210 is an advanced X-ray Absorption Spectroscopy (XAS) system designed to deliver exceptional performance. With its high resolution and sensitivity, this system provides detailed elemental and chemical state analysis.

The QuantumLeap-V210 offers synchrotron-like performance in a laboratory setting, making it an invaluable tool for researchers. Additionally, it supports both fluorescence and transmission modes, covering a broad energy range for comprehensive analysis. Whether for life sciences, environmental studies, or materials science, the SIGRAY QuantumLeap-V210 ensures precise and reliable results.

Features of SIGRAY QuantumLeap-V210

Only laboratory XAS system with synchrotron-like performance

XANES at 0.7eV and EXAFS within seconds or minutes

2.1keV to 10keV, enabling low atomic number element analysis

Down to 2.1 keV for phosphorus and sulfur analysis within the vacuum enclosure

MicroXAS at 100 micron spot size

Motorized stage enables XAS mapping at 100 µm over a sample for microXANES and microEXAFS

Patented QuantumLeap-V210 Acquisition Scheme for Precise XAS Spectrum Imaging

Patented QuantumLeap-V210 acquisition scheme. A focusing X-ray optic directs X-rays onto the sample. A downstream crystal separates the transmitted X-rays by wavelengths into different positions on the spatially resolving detector. The resulting “image” by the detector is the XAS spectrum.

Intuitive Workflow and Real-Time Spectrum Display with QuantumLeap Software

QuantumLeap software follows an intuitive workflow in which the element of interest is selected and suggested settings are loaded. Options such as exposure times and number of images are then input. The acquired spectrum is displayed in real time during collection.

Achieving a Smooth Spectrum for XAS with Mo and W Target Materials in QuantumLeap-V210

Mo (blue) has characteristic X-ray lines around 2 to 3 keV and 17.4 keV, while W (green) has characteristic energies in the 7 to 12 keV range. By selecting target materials, characteristic lines can be avoided so that a smooth spectrum of energies is acquired for a full range between 4.5 to 25 keV.

Application

  • Catalysts
  • Batteries and Fuel Cells
  • Nanoparticles and Nanotubes

Analysis of chemistry in a Co-Cu catalyst sample and measurement of a reference Co foil. Note high resolution features such as pre-edges can be clearly seen.

XANES spectrum of a new versus aged lithium ion battery cathode, demonstrating chemical changes.

Hematite and magnetite iron nanopowder XANES analysis.

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